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100°C NaOH J Org Chem, (19841, 3,892 67% a q . NaOH C1 2C=CHS02"Bu H02CCH2S02~Bu 80% Mirskova, A . N . G. -J Org Chem USSR, (19841, -- Guseva, M , 545 SECTION 30: Acid Derivatives from Miscellaneous Canpounds 1 . LiAlH. 4 CP I 2 . CO/Ag'/THF 3. 4 BH3-THF ,F e, Me3 p"' I CO "- c o * 4. repeat 2-3, twice 5 . a q . G. K. Synthesis, ( 1 9831, 605 SECTION 3OA: Protection of Carboxylic Acid Derivatives O C O O H I Boc - 9 - f 1 u o r e n y l met h a n o l DCCy DMAP 6 0 % B'o c DEA , RT * Kessler, H.

Tetrahedron E ,( 1 9851, 96% 26, 681 50 COMPENDIUM OF ORGANIC SYNTHETIC METHODS VOL 6 SECTION 45A quant. Boeckman J r . F. HO Potenza, J . C . C. * Related Methods: l h 54% Syn Cornnun, (1986), 16, 111 Esters from Alcohols (Section 123) Alcohols from Ethers (Section 39) Esters from Alcohols (Section 108) Alcohols from Esters (Section 38) Compendium of Organic Synthetic Methods, Volume 6 Edited by Michael B. Smith Copyright 0 1988 by John Wiley & Sons, Inc. CHAPTER 4 PREPARATION OF ALDEHYDES SECTION 46: Aldehydes Acetylenes No Additional Examples SECTION --+Derivatives 3: Adehydes from Acid (LCOOH L 1 .

Guindon, Y. 26, aq. NaHC03 1. nBu4NF/THF, 2. aq. )f;ioQJoH / - 96% 0°C NH4C1 * Flinch, H. J. Tetrahedron E ,( 1 9851, 96% 26, 681 50 COMPENDIUM OF ORGANIC SYNTHETIC METHODS VOL 6 SECTION 45A quant. Boeckman J r . F. HO Potenza, J . C . C. * Related Methods: l h 54% Syn Cornnun, (1986), 16, 111 Esters from Alcohols (Section 123) Alcohols from Ethers (Section 39) Esters from Alcohols (Section 108) Alcohols from Esters (Section 38) Compendium of Organic Synthetic Methods, Volume 6 Edited by Michael B.

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