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By Bernard D. Blaustein, Bradley C. Bockrath, and Sidney Friedman (Eds.)

content material: Small-angle X-ray research of the porosity in coals / M. Kalliat, C.Y. Kwak, and P.W. Schmidt --
Carbon-13 CP/MAS examine of coal macerals of various rank / Ronald J. Pugmire, Kurt W. Zilm, David M. supply, Stephen R. Larter, James Allen, Joseph T. Senftle, Alan Davis, and William Spackman --
Cross-linked buildings in coals : versions and initial experimental info / Lucy M. Lucht and Nikolaos A. Peppas --
Coal constitution and thermal decomposition / Peter R. Solomon --
The interrelationship of graphite intercalation compounds, ions of fragrant hydrocarbons, and coal conversion 2 / Lawrence B. Ebert, Joseph C. Scanlon, Daniel R. turbines, and Louis Matty --
A research of coal oxidation via charged-particle activation research / D.J. Schlyer and A.P. Wolf --
A primary chemical kinetics method of coal conversion / Stephen E. Stein --
Short-contact-time coal liquefaction : influence of coal rank and solvent resource on conversions and heptane-insoluble product compositions / James R. Longanbach --
The influence of solvent compositions at the liquefaction habit of Western subbituminous coal / L.R. Rudnick and D.D. Whitehurst --
interplay of naphthalene with bituminous coal : an EPR and NMR research / Joseph J. Ratto and Ira B. Goldberg --
Coal mineral subject catalysis in liquefaction / Bradley C. Bockrath and Karl T. Schroeder --
The kinetics of flash hydrogenation of lignite and subbituminous coal / B.L. Bhatt, P.T. Fallon, and M. Steinberg --
features of coal-derived drinks from diversified tactics : relationships to coal constitution / Larry L. Anderson, Kwang E. Chung, Ronald J. Pugmire, and Joseph Shabtai --
Dialytic extraction of coal and its program to the research of metals speciation / Dennis H. Finseth, Bernard J. Porzucek, and Richard G. Lett --
Characterization of coal-derived fabrics through matrix isolation spectroscopy / E.L. Wehry and Gleb Mamantov --
research of synfuels through MS/MS / D. Zakett and R.G. chefs --
600-MHz proton magnetic resonance learn of coal-derived drinks / T. Hara, N.C. Li, K.C. Tewari, and F.K. Schweighardt --
Coal liquid upgrading utilizing metallophthalocyanine catalysts : hydrogenation of the version compound quinoline / L.J. Boucher, N.L. Holy, and B.H. Davis --
examine within the electrochemistry of coal-derived drinks / James B. Pierce --
The Fe-S-O-H approach lower than coal liquefaction stipulations / W.D. Richey --
Mössbauer research of the transformation of iron minerals in the course of coal conversion / P.A. Montano, V. Shah, S. Reddy, and A.S. Bommannavar --
a brand new procedure for research of pyrite in coal and lignite / M. Hyman and M.W. Rowe --
overview of the elimination of natural sulfur from coal / R. Markuszewski, L.J. Miller, W.E. Straszheim, C.W. Fan, T.D. Wheelock, and R.T. Greer --
Thermal oxidative degradation of coal as a path to sulfur performance : an preliminary examine / Robert B. Lacount, Douglas okay. Gapen, Winson P. King, David A. Dell, Fred W. Simpson, and Charles A. Helms --
source improvement within the analytical chemistry of sulfur compounds for the recent coal conversion applied sciences / Joseph Jordan, S.J. Ankabrandt, A. Robbat, and J.D. Stutts.

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By Bernard D. Blaustein, Bradley C. Bockrath, and Sidney Friedman (Eds.)

content material: Small-angle X-ray research of the porosity in coals / M. Kalliat, C.Y. Kwak, and P.W. Schmidt --
Carbon-13 CP/MAS examine of coal macerals of various rank / Ronald J. Pugmire, Kurt W. Zilm, David M. supply, Stephen R. Larter, James Allen, Joseph T. Senftle, Alan Davis, and William Spackman --
Cross-linked buildings in coals : versions and initial experimental info / Lucy M. Lucht and Nikolaos A. Peppas --
Coal constitution and thermal decomposition / Peter R. Solomon --
The interrelationship of graphite intercalation compounds, ions of fragrant hydrocarbons, and coal conversion 2 / Lawrence B. Ebert, Joseph C. Scanlon, Daniel R. turbines, and Louis Matty --
A research of coal oxidation via charged-particle activation research / D.J. Schlyer and A.P. Wolf --
A primary chemical kinetics method of coal conversion / Stephen E. Stein --
Short-contact-time coal liquefaction : influence of coal rank and solvent resource on conversions and heptane-insoluble product compositions / James R. Longanbach --
The influence of solvent compositions at the liquefaction habit of Western subbituminous coal / L.R. Rudnick and D.D. Whitehurst --
interplay of naphthalene with bituminous coal : an EPR and NMR research / Joseph J. Ratto and Ira B. Goldberg --
Coal mineral subject catalysis in liquefaction / Bradley C. Bockrath and Karl T. Schroeder --
The kinetics of flash hydrogenation of lignite and subbituminous coal / B.L. Bhatt, P.T. Fallon, and M. Steinberg --
features of coal-derived drinks from diversified tactics : relationships to coal constitution / Larry L. Anderson, Kwang E. Chung, Ronald J. Pugmire, and Joseph Shabtai --
Dialytic extraction of coal and its program to the research of metals speciation / Dennis H. Finseth, Bernard J. Porzucek, and Richard G. Lett --
Characterization of coal-derived fabrics through matrix isolation spectroscopy / E.L. Wehry and Gleb Mamantov --
research of synfuels through MS/MS / D. Zakett and R.G. chefs --
600-MHz proton magnetic resonance learn of coal-derived drinks / T. Hara, N.C. Li, K.C. Tewari, and F.K. Schweighardt --
Coal liquid upgrading utilizing metallophthalocyanine catalysts : hydrogenation of the version compound quinoline / L.J. Boucher, N.L. Holy, and B.H. Davis --
examine within the electrochemistry of coal-derived drinks / James B. Pierce --
The Fe-S-O-H approach lower than coal liquefaction stipulations / W.D. Richey --
Mössbauer research of the transformation of iron minerals in the course of coal conversion / P.A. Montano, V. Shah, S. Reddy, and A.S. Bommannavar --
a brand new procedure for research of pyrite in coal and lignite / M. Hyman and M.W. Rowe --
overview of the elimination of natural sulfur from coal / R. Markuszewski, L.J. Miller, W.E. Straszheim, C.W. Fan, T.D. Wheelock, and R.T. Greer --
Thermal oxidative degradation of coal as a path to sulfur performance : an preliminary examine / Robert B. Lacount, Douglas okay. Gapen, Winson P. King, David A. Dell, Fred W. Simpson, and Charles A. Helms --
source improvement within the analytical chemistry of sulfur compounds for the recent coal conversion applied sciences / Joseph Jordan, S.J. Ankabrandt, A. Robbat, and J.D. Stutts.

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Due to the porous s t r u c t u r e of the c o a l samples not a l l the imbibed s w e l l i n g agent c o n t r i b u t e d to the c o a l s w e l l i n g . A c o n s i d e r a b l e p o r t i o n of t h i s solvent American Chemical Society Library 1155 16th St. N. w. ; ACS Symposium Series; Washington, American 0. Chemical C. Society: 2 0 0 3 6 Washington, DC, 1981. ; ACS Symposium Series; American Chemical Society: Washington, DC, 1981. 89 57 50 25 20-30 30-40 30-40 57 57 50 25 20-30 30-40 30-40 20-30 57 50 25 20-30 30-40 30-40 57 50 25 57 50 25 20-30 30-40 30-40 20-30 30-40 30-40 57 50 25 20-30 30-40 30-40 Only the 20-30 mesh c o a l s were e x t r a c t e d before s w e l l i n g .

Sample Separation and C h a r a c t e r i z a t i o n . Three v i t r i n i t e samples ( S i l k s t o n e , High Hazels, and W e s t f i e l d ) were obtained by hand-picking of macroscopic v i t r a i n bands i n Carboniferous c o a l s . Selected v i t r a i n p a r t i c l e s were crushed to pass a B. S. 100 mesh s i e v e (250 μ) and p o l i s h e d mounts were prepared. Sample p u r i t y was determined by p o i n t - c o u n t i n g (sample r e f l e c t i v i t y ) 500 p o i n t s , g i v i n g a ± 2% (by volume) accuracy (18).

Ch003 V K m/p+m/p c c s s K ' K Here m, ρ and V denote weight, d e n s i t y and volume o f the two com­ ponents, i . e . c o a l and s w e l l i n g agent, which are designated by the s u b s c r i p t s c and s r e s p e c t i v e l y ; then V designates the volume o f the swollen c o a l . An apparent volume degree o f s w e l l i n g , Q pp, can a l s o be determined from equation (6). g a Q = 1/U app 2,app (6) 0 x Accurate determination of the c o a l volume f r a c t i o n i n the swollen c o a l p a r t i c l e s can be done by c a l c u l a t i n g and excluding the pore volume, Vp, occupied by the solvent during s w e l l i n g .

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