By Hans-Josef Altenbach, Hans-Ulrich Reißig, Karsten Krohn, Manfred Braun, Johann Mulzer
This strange choice of forty nine essays offers an outline of the traits and accomplishments of artificial natural chemistry lately. specific in its technique, it offers with virtually each element of contemporary synthesis.
the 1st a part of the e-book describes equipment and reagents, with specific emphasis on swiftly constructing organometallic and biooriented approaches. within the moment half, those instruments are utilized to the syntheses of attention-grabbing aim compounds and common compounds with notable physiological houses. Mechanistic discussions and retrosynthetic analyses are integrated. greater than a thousand up to date references support the reader to pursue the themes highlighted right here.
This publication offers either the lively researcher and the complex scholar perception into the aggressive surroundings, creativity, and resourcefulness so attribute of natural synthesis at the present time
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Extra info for Organic Synthesis Highlights v. 1
D. Stringer, R. H. , and F. A. Davis, Tetrahedron Lett. 22, 4385 (1981). 44 Stereodifferentiating Addition Reactions [ll] F. A. Davis. M. S. Haque. G. Ulatowski, and J. C. Towson, J. Org. Chem. 51, 2402 (1986).  F. A. Davis and M. S. Haque, J. Org. Chem. 51, 4083 (1986).  F. A. Davis, A. C. Sheppard, and G. S. Lal, Tetrahedron Lett. 30,779 (1989).  F. A. Davis, M. S. Hague, and R. M . Przeslawski, J. Org. Chem. 54, 2021 (1987). [l5] F. A. Davis, T. G. Ulatowski, and M. S. Haque, J .
Chim. Acta 67, 1562 (1984).  S. E. Denmark, M . S. Dappen, and C. J. Cramer, J . Am. Chem. SOC. 108, 1306 (1986). [I81 E. J. Corey, B. Samuelsson, and F. A. Luzzio, J. Am. Chem. 106, 3682 (1984). Organic Synthesis Highlights Edited by J. -J. Altenbach, M. Braun, K. -U. Reissig OVCH Verlagsgesellschaft mbH, 1991 Boron: Reagents for Stereoselective Syntheses Diborane, BzH6,once a chemical curiosity, has developed into an extremely useful reagent, especially since chemists have learned to apply it in its various modified fbrms.
This is particularly true for enantiomerically pure cyclic acetals involved in asymmetric syntheses. Because of the rigid stereochemistry characterizing the heterocyclic acetal ring, stereoselectivity is not restricted only to the ring, but may under some conditions apply to reactions at distant sites, or to the acetal center itself. It is the latter case that appears to be most useful and interesting, since Lewis acid-catalyzed substitution at the acetal function permits C-C bond formation with a variety of carbon nucleophiles.